This is where IoT joins Chemistry
IoT-based Electrosynthesis ecosystem
Using MQTT over WiFi
In this proposal we presented the electrosynthesis ecosystem using esp8266 with OTA compilation integrated, the MQTT Broker for the control system that would be installed on a Raspberry Pi and MQTT protocol for the wireless data transfer layer which provides the electrosysnthesis machine to work 24/7 and with the AI that can be implemented, the whole ecosystem would be smart and the data-driven can be used in QC verification. This system is designed and simulated and the source codes are available via GitHub.
IoT-based Electrosynthesis Machine
Green & Solar-powered None-catalyst
According to the conclusion of referenced article, None-catalyst and clean synthesis of symmetric and asymmetric indoles from electrochemical oxidation of 4-aminophenol in the presence of malononitrile in green media ; we are trying to integrate Internet of Things (IoT) with electrochemical synthesis under controlled potential conditions in order to use green solvent instead of organic materials, and create a solar-powered 24/7 automated machine for the industrial use cases.
Green and one-pot electrosynthesis
of a new amino benzofuran
Electrochemical oxidation of 1,4-dihydroxyanthraquinone has been studied in the presence of malononitrile as a nucleophile in acetate buffer solution mixed with ethanol (40/60 v/v) using cyclic voltammetry and coulometry under constant potential methods. The results revealed that tetra-one derived from electrochemical oxidation of 1,4-dihydroxyanthraquinone can be participates in 1,4-Michael addition reaction with malononitrile. The formed adducts convert to the corresponding benzofuran via ECC (Electrochemical, chemical, chemical reactions) mechanism.